The mixture was stirred at 7O 0 C overnight and filtered through Celite.(R).. The colourless filtrate was concentrated and acidified with HCl (aq., 2M). Filtration gave the title compound as a white powder which was used without further purification. (Yield: 913 mg 5 80percent). 1 H-NMR (DMSO-d 6): δ 6.80 (s, IH) 5 4.40 (br s, IH). 67%

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Often, holes are collared with RC equipment until the hole is almost in the zone, and then changed over to diamond core. Some are cored for the entire length. Core size is HQ (63.5 mm core diameter), sometimes reduced to NQ (47.6 mm core diameter). RC holes are drilled with 146 mm diameter equipment, which produces a hole approximately 152 mm ...

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